NMR
This facility was funded by DST through FIST programme. At present, the facility has Bruker Avance 400 MHz and Bruker Avance 500MHz FT-NMR spectrometers for internal as well as external use. The instruments have the following features
- 400 MHz FT-NMR Spectrometer. Probe: 5mm BBO probe for solution studies.
- 500 MHz FT-NMR Spectrometer. Probe: 5mm BBI probe for solution studies.
- Software: Bruker Topspin.
- VT Accessory: Variable temperature facility is available from RT to +130 degree with suitable solvent.
Service Charges for NMR Spectral Measurements
| S.No. | Solvent | Nuclei | External Samples (Per sample per nucleus) | |||
|---|---|---|---|---|---|---|
| 400Mhz | 500Mhz | |||||
| Academic Rs. | Industry Rs. | Academic Rs. | Industry Rs. | |||
| 1 | Chloroform CDCl3 |
1H, 19F, 31P, 13C | 200 | 400 | 300 | 600 |
| 2 | Dimethyl sulfoxide DMSO-D6 |
1H, 19F, 31P, 13C | 450 | 900 | 500 | 1000 |
| 3 | Water D2O |
1H, 19F, 31P, 13C | 200 | 400 | 300 | 600 |
| 4 | Acetone (CD3)2CO |
1H, 19F, 31P, 13C | 400 | 800 | 500 | 1000 |
| 5 | Other nuclei, DEPT, 2D and special experiments | 500 | 1000 | 600 | 1200 | |
| 6 | For other solvents, conntact staff in-charge | |||||
Sample submission: Sample must be submitted either through post or in person along with duly completed requisition form and payment details.
Sample requirement: Kindly make sure that your sample (10 mg for 1H, 19F, 31P NMR and 30 mg for 13C, 15N NMR) is soluble in 0.5 mL of required solvent completely (clear solution)
Mode of Payment: Refer “Service Requisition Form”
Staff in-charge Contact E-mail: nmrchemgri@gmail.com
Downloads:
Click here to download Service Requisition Form (Internal)
TGA/DTA
Make : NETZSCH
Model : NJA – STA 2500 Regulus
Software: Proteus
Service Charges for TGA/DTA Analysis
| S.No. | Details | ||||
|---|---|---|---|---|---|
| Temperature ranges | 30 - 500oC | 30 - 800oC | 30 - 1000oC | 30 - 1250oC | |
| 1 | External Fee Academic (Rs.) | 500 | 750 | 1000 | 1250 |
| 2 | External Fee Industry (Rs.) | 1000 | 1500 | 2000 | 2500 |
Sample submission: Sample must be submitted either through post or in person along with duly completed requisition form and payment details
Mode of Payment: Refer “Service Requisition Form”
TGA/DTA will be recorded only after the payment
Staff in-charge Contact E-mail: tgachemgri@gmail.com
Payment details
1. Challan through Canara Bank at Gandhigram Rural Institute Branch (Original office copy of the challan must be submitted)
2. Demand Draft: Payable in favor of
"IACCProf and Head, Department of Chemistry,
Gandhigram Rural Institute - Deemed to be University,
Gandhigram - 6243 02
Downloads:
UV-Vis Spectrometer
Make : Perkin Elmer
Model : Perkin Elmer LAMBDA – 35
Service Charges for UV–Vis Spectroscopy Analysis
| S.No. | Details | Amount (Rs.) per sample |
|---|---|---|
| 1 | External Fee Academic (Rs.) | 50 |
| 2 | External Fee Industry (Rs.) | 100 |
Sample submission: Sample must be submitted either through post or in person along with duly completed requisition form and payment details
Mode of Payment: Refer “Service Requisition Form”
UV-Vis spectroscopy analysis will be recorded only after the paymentPayment details
1. Challan through Canara Bank at Gandhigram Rural Institute Branch (Original office copy of the challan must be submitted)
2. Demand Draft: Payable in favor of
"IACCProf and Head, Department of Chemistry,
Gandhigram Rural Institute - Deemed to be University,
Gandhigram - 6243 02
Downloads:
FT-IR Spectrometer
Make : Jasco
Model : FT/IR – 4700
Service Charges for FT–IR Analysis
| S.No. | Details | Amount (Rs.) per sample |
|---|---|---|
| 1 | External Fee Academic (Rs.) | 75 |
| 2 | External Fee Industry (Rs.) | 150 |
Sample submission: Sample must be submitted either through post or in person along with duly completed requisition form and payment details
Mode of Payment: Refer “Service Requisition Form”
FT–IR analysis will be recorded only after the paymentPayment details
1. Challan through Canara Bank at Gandhigram Rural Institute Branch (Original office copy of the challan must be submitted)
2. Demand Draft: Payable in favor of
"IACCProf and Head, Department of Chemistry,
Gandhigram Rural Institute - Deemed to be University,
Gandhigram - 6243 02
Downloads:
Atomic Absorption Spectrometer
Make : Perkin Elmer
Model : Perkin Elmer A Analyst 100
Service Charges for Atomic Absorption Spectroscopy (AAS) Analysis
| S.No. | Details | Amount (Rs.) per Element per sample |
|---|---|---|
| 1 | External Fee Academic (Rs.) | 100 |
| 2 | External Fee Industry (Rs.) | 200 |
Element analysis: Cr, Cu, Fe, Zn, Mn, Pb and As only
Condition: Samples must be completely dissolved in water (H2O) (Clear solution)
Sample submission: Sample must be submitted either through post or in person along with duly completed requisition form and payment details
Mode of Payment: Refer “Service Requisition Form”
AAS analysis will be recorded only after the paymentPayment details
1. Challan through Canara Bank at Gandhigram Rural Institute Branch (Original office copy of the challan must be submitted)
2. Demand Draft: Payable in favor of
"IACCProf and Head, Department of Chemistry,
Gandhigram Rural Institute - Deemed to be University,
Gandhigram - 6243 02
